New compound



Patented lV lar.2 O,194 5 i UNITED STATES PATENT OFFICE Corporation, Akron, Ohio, a corporation of Delaware No Drawing. Application October 3, 1942,

Serial N0. 460,652

1 Claim. (01. 260592) This invention relates to alpha, alpha, beta grams of alpha, alpha, beta trichloropropionyl trichloropropiophenone. The preparation of the chloride. Immediately the solution warmed,

compound is illustrated 'by the following forn to stand overnight, and then the solution was evolved H01, and became dark, This was allowed mula: y

( C1 01 Cl 5 hydrolyzed with ice-cold dilute aqueous HCl.

1 1 l The benzene layer was separated and distilled. m fi There was obtained a good yield of alpha, alpha,

0 01 H a 0 01 H beta trichloropropiophenone, boiling point170- 172 C./38 mm.; N =1.523 l r 10 What I claim is: To a mixture of 70 grams of anhydrous AlCla Alpha, alpha, beta trichloropropiophenone. and 300 cc. of anhydrous benzene was added 98 n JOY G. LICHTY. 

